- 作者: Rashed, N. ; Sayed, M. ; El Ashry, E.S.H.
- 作者服務機構: Chemistry Dept., Alexandria Univ., Alexandria, Egypt
- 中文摘要: Several linearly fused tricyclic 6,7,6-systems were prepared. Reaction of 1,2-diamino-4-nitrobenzene with 5,5- dimethylcyclohexan-1,3-dione gave 3-(2-amino-5-nitroanilino)-5,5-dimethylcyclohex-2-en-1-one (8). Reaction of 8 and its analogue with various aldehydes gave 2,3,4,5,10,11- hexahydro-3,3-dimethyl-11-substituted-1H-dibenzo [ b,e ] [ 1,4 ] diazepin-1-ones 9 and 10. Acetylation of 9 and 10 gave the corresponding N-acetyl derivatives. Spectral data of the products are discussed.
- 英文摘要: --
- 中文關鍵字: Acetylation; 1,2-Diamino-4-Nitrobenzene; 5,5- Dimethylcyclohexane-1,3-Dione; N-Acetyl Derivative; Synthesis
- 英文關鍵字: 乙醯化;1;2-二氨基-4-硝基苯;5;5-二甲基環陸烷-1;3-雙酮;氮-乙醯基衍生物;合成