- 作者: Yah-Ping Liu and Wu-Hsiung Ho
- 中文摘要: The solid-phase microextraction (SPME) technique using a 100 m film polydimethylsiloxane (PDMS) coated fiber has been examined with the aim to determine dichlorobenzene in aqueous samples. The feasibility of SPME-GC-ECD analysis has been evaluated. Absorption time of 30 min was selected and 1 min was long enough for complete desorption of the analytes in the injection port of the gas chromatograph. Linear ranges from 0.03 to 5 g/L and method detection limits between 7 and 9 ng/L for dichlorobenzenes were obtained. The relative standard deviations were less than 12% for a spiking level of 3 g/L. The proposed method was applied to determine dichlorobenzenes in spiked deionized water, ground water, and in industrial effluent samples.
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